QIU Rong, FAN Weicheng, CHEN Jun. PREPARATION OF EPA AND DHA ESTERS WITH HIGH PURITY BY SUPERCRITICAL CO2 EXTRACTION AND RECTIFICATION[J]. CIESC Journal, 2001, (5).
QIU Rong, FAN Weicheng, CHEN Jun. PREPARATION OF EPA AND DHA ESTERS WITH HIGH PURITY BY SUPERCRITICAL CO2 EXTRACTION AND RECTIFICATION[J]. CIESC Journal, 2001, (5).DOI:
超临界CO2萃取精馏制取高纯度EPA乙酯和DHA乙酯
摘要
Abstract
Fish oil ethyl esters complexed with aqueous silver nitrate solution were extracted and rectified by supercritical CO2 to obtain DHA ester and EPA ester with high purity. The effects of some independent variables
such as extraction pressure
temperature gradient of rectifying column and programmed pressure
on rectification were investigated.The results showed that programmed pressure is suitable for purification of EPA and DHA esters. Increase of column temperature gradient from bottom to top is one of the key elements in rectification. Furthermore
higher temperature gradient leads to better separation effect.