WANG Ben, CAO Yan, HUANG Kelin, et al. Dissolution and regeneration of sugarcane bagasse cellulose in ionic liquid[J]. CIESC Journal, 2010, (6): 1592-1598.
WANG Ben, CAO Yan, HUANG Kelin, et al. Dissolution and regeneration of sugarcane bagasse cellulose in ionic liquid[J]. CIESC Journal, 2010, (6): 1592-1598.DOI:
Regenerated cellulose film is prepared successfully from sugarcane bagasse cellulose in ionic liquid 1-allyl-3-methylimidazolium chloride ([Amim]Cl).Its dissolution process was viewed by polarizing microscope.Properties and structures of the regenerated cellulose films obtained were characterized by infrared spectroscopes
scanning electron microscopy
X-ray diffraction
thermogravimetry (TGA) and strength test.The results showed that [Amim]Cl is a good non-derivatizing solvent for sugarcane bagasse cellulose whose crystalline form transformed completely from cellulose Ⅰ to cellulose Ⅱ after regenerated directly from [Amim]Cl solution.The cellulose film obtained by regeneration showed a dense structure and its thermal stability and tensile strength could be up to 292℃ and 144 MPa respectively.