Preparation and modification of nano-ZnO/CeO<sub>2</sub> composite oxides

LI Xiuping; ZHAI Yuchun; MA Peihua; ZHAO Rongxiang; LI Lihua; ZHANG Jinsheng

doi:10.3969/j.issn.0438-1157.2013.08.050

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Preparation and modification of nano-ZnO/CeO₂ composite oxides

更新时间：2025-12-10

- Preparation and modification of nano-ZnO/CeO₂ composite oxides
- CIESC Journal Issue 8, Pages: 3054-3061(2013)
- 作者机构：
  
  1. 东北大学材料与冶金学院,辽宁,沈阳,110004
  2. 辽宁石油化工大学化学化工与环境学部,辽宁,抚顺,113001
- 作者简介：
- 基金信息：
- DOI：10.3969/j.issn.0438-1157.2013.08.050
  CLC： 614.33
- Online First：05 August 2013，
  
  Published：05 August 2013
- 稿件说明：
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LI Xiuping, ZHAI Yuchun, MA Peihua, et al. Preparation and modification of nano-ZnO/CeO₂ composite oxides[J]. CIESC Journal, 2013, (8): 3054-3061. DOI: 10.3969/j.issn.0438-1157.2013.08.050.
DOI：

LI Xiuping, ZHAI Yuchun, MA Peihua, et al. Preparation and modification of nano-ZnO/CeO₂ composite oxides[J]. CIESC Journal, 2013, (8): 3054-3061. DOI: 10.3969/j.issn.0438-1157.2013.08.050. DOI：

摘要

以燃烧法制备氧化锌并以其为包裹对象用沉淀法合成ZnO/CeO2复合氧化物

采用XRD、SEM 、IR、TG-DTA、UV-Vis、TEM对样品进行表征

结果表明氧化铈以包覆形式与氧化锌形成复合氧化物。用改性剂对复合氧化物进行改性研究

以亲油化度考察改性剂的类型、改性剂的用量、改性温度、pH值对改性效果的影响。实验结果表明:当选用硬脂酸钠为改性剂且用量为ZnO/CeO2的4%

改性温度为60℃

pH值为7时

样品粒径明显变小

分散性变好

亲油化度明显提高

可获得最佳改性效果。

Abstract

Zinc oxide was prepared by the combustion method.ZnO/CeO2 composite oxides were synthesized by the precipitation method with zinc oxide as the coated object.The samples were characterized by XRD

SEM

TG-DTA

UV-Vis and TEM.ZnO was coated by CeO2 and composite oxides were formed.The composite oxides were modified with modifier reagent

and modification effect was evaluated by the degree of oil-affinity.The type of modifier

mass ratio of modifier

reaction temperature and pH value of solution were studied.The optimal reaction conditions were as follows:modifier stearate

temperature 60℃

mass ratio of modifier 4% of composite oxides

pH value of solution 7.Particle size became smaller

dispersion of samples was better and the degree of oil-affinity of sample was improved after the samples were modified.

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Preparation and modification of nano-ZnO/CeO2 composite oxides

DOI：10.3969/j.issn.0438-1157.2013.08.050

摘要

Abstract

关键词

Keywords

references

Preparation and modification of nano-ZnO/CeO₂ composite oxides