Solvent free synthesis of methyl dihydroxyethyl allyl ammonium chloride

MAO Taoyan; ZHENG Cheng; LIN Jing; CHEN Xiaoling; HUANG Xiaoluo; XING Xu; ZHANG Liping

doi:10.3969/j.issn.0438-1157.2013.05.052

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Solvent free synthesis of methyl dihydroxyethyl allyl ammonium chloride

更新时间：2025-12-10

- Solvent free synthesis of methyl dihydroxyethyl allyl ammonium chloride
- CIESC Journal Issue 5, Pages: 1884-1889(2013)
- 作者机构：
  
  1. 广西大学化学化工学院,广西,南宁,530004
  2. 广州大学精细化工研究所,广东,广州,510006
  3. 广州天赐有机硅科技有限公司,广东,广州,510660
- 作者简介：
- 基金信息：
- DOI：10.3969/j.issn.0438-1157.2013.05.052
  CLC： Q423.12
- Online First：05 May 2013，
  
  Published：05 May 2013
- 稿件说明：
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MAO Taoyan, ZHENG Cheng, LIN Jing, et al. Solvent free synthesis of methyl dihydroxyethyl allyl ammonium chloride[J]. CIESC Journal, 2013, (5): 1884-1889.
DOI：

MAO Taoyan, ZHENG Cheng, LIN Jing, et al. Solvent free synthesis of methyl dihydroxyethyl allyl ammonium chloride[J]. CIESC Journal, 2013, (5): 1884-1889. DOI： 10.3969/j.issn.0438-1157.2013.05.052.

摘要

Abstract

Methyl dihydroxyethyl allyl ammonium chloride(MDAAC)was synthesized from N-methyl diethanolamine( MDEA )and allyl chloride by the solvent-free synthesis method.The effects of reaction time

reaction temperature and reactant molar ratio on reaction conversion rate were studied.The optimum process of synthesizing MDAAC obtained by orthogonal experiment was 60 min reaction time

50℃ reaction temperature and 1∶1.3 molar ratio of MDEA and allyl chloride.The target product was purified by recrystallization and the yield of product was 97%.The structure of product was characterized by IR

1H NMR and 13C NMR.

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