Reaction of diaryl disulfides with nitroarenes

LI Shuyan; SUN Lina; SHEN Shujun; CHENG Tianxing; CHENG Shuanghua; CHEN Jiuxi

doi:10.11949/j.issn.0438-1157.20161755

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Reaction of diaryl disulfides with nitroarenes

更新时间：2025-12-10

- Reaction of diaryl disulfides with nitroarenes
- CIESC Journal Issue 6, Pages: 2394-2398(2017)
- 作者机构：
  
  1. 漳州职业技术学院食品与生物工程系,福建,漳州,363000
  2. 农产品深加工及安全福建省高校应用技术工程中心,福建,漳州,363000
  3. 温州大学化学与材料工程学院,浙江,温州,325035
- 作者简介：
- 基金信息：
- DOI：10.11949/j.issn.0438-1157.20161755
  CLC： 6
- Online First：05 June 2017，
  
  Published：05 June 2017
- 稿件说明：
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LI Shuyan, SUN Lina, SHEN Shujun, et al. Reaction of diaryl disulfides with nitroarenes[J]. CIESC Journal, 2017, (6): 2394-2398.
DOI：

LI Shuyan, SUN Lina, SHEN Shujun, et al. Reaction of diaryl disulfides with nitroarenes[J]. CIESC Journal, 2017, (6): 2394-2398. DOI： 10.11949/j.issn.0438-1157.20161755.

摘要

以二芳基二硫醚（ArSSAr）和硝基芳烃（ArNO2）为原料，在廉价易得的甲醛次硫酸氢钠（Rongalite®）和碳酸钾（K2CO3）共同促进下，以二甲亚砜（DMSO）为溶剂，50℃下合成了一系列非对称二芳基硫醚衍生物，产物结构经1H NMR和13C NMR确证。该方法具有反应条件温和、原料易得和操作简单等优点。

Abstract

The cheap and readily available Rongalite®/K2CO3 promoted the reaction of diaryl disulfides with nitroarenes in DMSO at 50 ℃

providing a convenient route to the synthesis of unsymmetrica diaryl sulfide. The structures of all products were characterized by 1H NMR and 13C NMR. This protocol had some distinct advantages of mild conditions

readily available starting materials and simple work-up.

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