HUANG Minhui, BAO Zongbi, DUAN Shuran, et al. Optimization of acid hydrolysis for preparing L-arabinose from Gum Arabic[J]. CIESC Journal, 2015, 66(7): 2528-2533.
DOI:
HUANG Minhui, BAO Zongbi, DUAN Shuran, et al. Optimization of acid hydrolysis for preparing L-arabinose from Gum Arabic[J]. CIESC Journal, 2015, 66(7): 2528-2533.DOI: 10.11949/j.issn.0438-1157.20150378.
Optimization of acid hydrolysis for preparing L-arabinose from Gum Arabic
当固液比为1:10 (g/ml)、100℃、0.1 mol·L-1 H2SO4水解90 min或90℃、0.1 mol·L-1 H2SO4水解200 min
水解液中L-阿拉伯糖的相对纯度分别达85%和87%
水解收率高达85%。
Abstract
Gum Arabic
an ideal raw material for preparing L-arabinose
can be catalytically hydrolyzed by sulfur acid to obtain the hydrolysate containing L-arabinose
D-galactose and L-rhamnose. In order to ensure the stability of subsequent purification process as well as product quality
optimization of the acid hydrolysis process is necessary. In this work
single factor experiments are performed to determine the key parameters of acid hydrolysis reaction. The effects of reaction time
acid concentration
temperature and solid-to-liquid ratio on the hydrolysis are investigated. The results show that the temperature affects more significantly on the yield rate of L-arabinose. The degree of hydrolysis as high as 85% and the relative purity of L-arabinose up to 85% or 87% can be obtained under the optimized hydrolysis conditions of 90 min reaction at 100℃ or 200 min reaction at 90℃ with 0.1 mol·L-1 H2SO4 and solid-to-liquid ratio of 1:10 (g/ml).