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1.浙江省化工高效制造技术重点实验室,浙江 杭州 310027
2.化学工程联合国家重点实验室,浙江 杭州 310027
3.浙江大学化学工程与生物工程学院,浙江 杭州 310027
Received:05 May 2019,
Revised:2019-06-05,
Online First:24 July 2026,
Published:05 October 2019
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黄正梁, 郭晓云, 帅云, 杨遥, 孙婧元, 蒋斌波, 王靖岱, 阳永荣. 射流鼓泡反应器内气液分散状态检测[J]. 化工学报, 2019, 70(10): 3906-3913
HUANG Zhengliang, GUO Xiaoyun, SHUAI Yun, YANG Yao, SUN Jingyuan, JIANG Binbo, WANG Jingdai, YANG Yongrong. Detection of gas-liquid dispersion in jet bubbling reactor[J]. CIESC Journal, 2019, 70(10): 3906-3913
黄正梁, 郭晓云, 帅云, 杨遥, 孙婧元, 蒋斌波, 王靖岱, 阳永荣. 射流鼓泡反应器内气液分散状态检测[J]. 化工学报, 2019, 70(10): 3906-3913 DOI: 10.11949/0438-1157.20190460.
HUANG Zhengliang, GUO Xiaoyun, SHUAI Yun, YANG Yao, SUN Jingyuan, JIANG Binbo, WANG Jingdai, YANG Yongrong. Detection of gas-liquid dispersion in jet bubbling reactor[J]. CIESC Journal, 2019, 70(10): 3906-3913 DOI: 10.11949/0438-1157.20190460.
射流鼓泡反应器内随着射流速度的增大,先后经历气泛、载气和完全分散三种气液分散状态。本文在射流鼓泡反应器实验装置中,利用Pavlov管测量气体分布器上方壁面附近的液速波动信号,发现液速标准差和时均液速随射流速度的增大均依次出现第一平稳段、上升段、下降段和第二平稳段,其中,第一平稳段对应气泛状态,上升和下降段对应载气状态,第二平稳段对应完全分散状态。据此提出了临界射流速度的判断准则:第一平稳段与快速上升段的交点对应的射流速度为泛点射流速度
u
jf
,下降段与第二平稳段的交点对应的射流速度为完全分散射流速度
u
jcd
。与目测法相比,液速标准差分析得到的
u
jf
的平均相对偏差为5.82%,
u
jcd
的平均相对偏差为18.2%;时均液速分析得到的
u
jf
的平均相对偏差为5.86%,
u
jcd
的平均相对偏差为12.1%。研究还发现泛点射流速度随表观气速的增大而增大。
In the jet bubbling reactor
as the liquid jet velocity increases
the gas-liquid dispersion shows three states including the flooding
loading
and complete dispersion. In this work
the liquid velocity near the wall above the gas distributor of the jet bubbling reactor was measured by the Pavlov tube to identify the aforementioned three dispersion states. It was found that the standard deviation of liquid velocity and the average liquid velocity both appeared four stages with the increase of jet velocity
which included the first plateau
the ascending stage
descending stage and second plateau. Wherein
the first plateau corresponded to the flooding state
the ascending and descending stages corresponded to the loading state
and the second plateau corresponded to the complete dispersion state. Therefore
the criterion for the critic
al jet velocity was proposed. The jet velocity at the intersection of the first plateau and the ascending stage was the flooding velocity
u
jf
and the jet velocity at the intersection of the descending stage and the second plateau was the complete dispersion velocity
u
jcd
. Compared with the visual observation method
the average relative deviation of
u
jf
obtained by liquid velocity standard deviation analysis was 5.82%
the average relative deviation of
u
jcd
was 18.2%; the average relative deviation of
u
jf
obtained by time-averaged liquid velocity analysis was 5.86%
and the average relative deviation of
u
jcd
was 12.1%. The study also found that the blunt jet velocity increases as the superficial gas velocity increases.
Amiri T Y , Moghaddas J S , Moghaddas Y . A jet mixing study in two phase gas–liquid systems [J ] . Chemical Engineering Research and Design , 2011 , 89 ( 3 ): 352 - 366 .
Huang Z L , Wang H T , Shuai Y , et al . Hydrodynamics in a jet bubbling reactor: experimental research and mathematical modeling [J ] . AIChE Journal , 2018 , 64 ( 5 ): 1814 - 1827 .
郭天琪 , 黄正梁 , 王靖岱 , 等 . 射流鼓泡反应器的混合特性 [J ] . 化工学报 , 2015 , 66 ( 11 ): 4438 - 4445 .
Guo T Q , Huang Z L , Wang J D , et al . Mixing characteristics in jet bubbling reactor [J ] . CIESC Journal , 2015 , 66 ( 11 ): 4438 - 4445
陈迎 . 射流鼓泡反应器中液相体积传质系数的测定 [J ] . 化学反应工程与工艺 , 2017 , 33 ( 3 ): 221 - 226 .
Chen Y . Mass transfer coefficient study of jet bubbling reactor [J ] . Chemical Reaction and Technology , 2017 , 33 ( 3 ): 221 - 226 .
黄正梁 , 帅云 , 杨遥 , 等 . 喷嘴结构对射流鼓泡反应器混合和传质性能的影响 [J ] . 化工学报 , 2018 , 69 ( 11 ): 4648 - 4654 .
Huang Z L , Shuai Y , Yang Y , et al . Effect of nozzle structure on the mixing and mass transfer characteristics in a jet bubbling reactor [J ] . CIESC Journal , 2018 , 69 ( 11 ): 4648 - 4654 .
Warmoeskerken M M C G , Smith J M . Flooding of disc turbines in gas-liquid dispersions: a new description of the phenomenon [J ] . Chemical Engineering Science , 1985 , 40 ( 11 ): 2063 - 2071 .
王凯 , 冯连芳 . 混合设备设计 [M ] . 机械工业出版社 , 2000 : 280 - 304 .
Wang K , Feng L F . Design of Mixing Equipment [M ] . Beijing : Mechanism Industry Press , 2001 : 280 - 304
Hills J H . Radial non-uniformity of velocity and voidage in a bubble column [J ] . Transactions of the Institution of Chemical Engineers , 1974 , 52 ( 1 ): 1 - 9 .
Forret A , Schweitzer J M , Gauthier T , et al . Influence of scale on the hydrodynamics of bubble column reactors: an experimental study in columns of 0.1, 0.4 and 1m diameters [J ] . Chemical Engineering Science , 2003 , 58 ( 3 ): 719 - 724 .
Gao Y , Hong D , Lu H , et al . Gas holdup and liquid velocity distributions in the up flow jet-loop reactor [J ] . Chemical Engineering Research and Design , 2018 , ( 136 ): 94 - 104 .
樊亚超 , 靳海波 , 秦岭 , 等 . 多级鼓泡塔内液体速度分布的实验研究 [J ] . 化学工程 , 2011 , 39 ( 10 ): 68 - 72 .
Fan Y C , Jin H B , Qin L , et al . Experimental study on liquid velocity distribution in multi-stage bubble column [J ] . Chemical Engineering(China) , 2011 , 39 ( 10 ): 68 - 72 .
Reimann J , Kusterer H , Jhon H . Two-phase mass flow rate measurements with Pitot tube and density measurements [C ] // Symp. Measuring Techniques in Gas-Liquid Two-Phase Flows . Nancy, France , 1983 .
Lee T H , Park G C , Lee D J . Local flow characteristics of subcooled boiling flow of water in a vertical concentric annulus [J ] . International Journal of Multiphase Flow , 2002 , 28 ( 8 ): 1351 - 1368 .
Franz K , Boerner T , Kantorek H J , et al . Flow structures in bubble columns [J ] . Gerchemeng , 1984 , 7 ( 6 ): 365 - 374 .
Drahoš J , Bradka F , Punčoch Ř M . Fractal behavior of pressure fluctuations in a bubble column [J ] . Chemical Engineering Science , 1992 , 47 ( 15 / 16 ): 4069 - 4075 .
Menzel T , in der Weide T , Staudacher O , et al . Reynolda shear stress for modeling of bubble column reactors [J ] . Industrial & Engineering Chemistry Research , 1990 , 29 ( 6 ): 988 - 994 .
于佩潜 , 门卓武 , 卜亿峰 , 等 . 多相流反应器流体力学参数测试技术进展 [J ] . 化工学报 , 2013 , 64 (S 1 ): 8 - 20 .
Yu P Q , Men Z W , Bu Y F , et al . Progress in measuring techniques of hydrodynamic parameters on multi-phase flow reactors [J ] . CIESC Journal , 2013 , 64 (S 1 ): 8 - 20 .
Kulkarni A A , Joshi J B , Kumar V R , et al . Application of multiresolution analysis for simultaneous measurement of gas and liquid velocities and fractional gas hold-up in bubble column using LDA [J ] . Chemical Engineering Science , 2001 , 56 ( 17 ): 5037 - 5048 .
刘友 , 杨晓涛 , 马修真 . 基于激光多普勒测速的流场测试技术 [J ] . 激光与红外 , 2012 , 42 ( 1 ): 18 - 21 .
Liu Y , Yang X T , Ma X Z . Application research progress of the multiphase flow measurement technology based on laser [J ] . Laser & Infrared , 2012 , 42 ( 1 ): 18 - 21 .
Vial C , Poncin S , Wild G , et al . Experimental and theoretical analysis of the hydrodynamics in the riser of an external loop airlift reactor [J ] . Chemical Engineering Science , 2002 , 57 ( 22 ): 4745 - 4762 .
Maru K , Hata T . Directional discrimination for fiber-optic non-mechanical scanning laser Doppler velocimeter using single transmission path [J ] . Optik - International Journal for Light and Electron Optics , 2014 , 125 ( 20 ): 6312 - 6314 .
Weigand P , Meier W , Duan X R , et al . Investigations of swirl flames in a gas turbine model combustor(Ⅰ): Flow field, structures, temperature, and species distributions [J ] . Combustion and Flame , 2006 , 144 ( 1 ): 205 - 224 .
郭文思 , 李龙国 , 刘超 , 等 . 淹没射流流场演化过程研究 [J ] . 工程科学与技术 , 2017 , 49 (Z 1 ): 35 - 43 .
Guo W S , Li L G , Liu C , et al . Study on the flow field of a submerged jet [J ] . Advanced Engineering Science , 2017 , 49 (Z 1 ): 35 - 43 .
Murai Y , Song X Q , Takagi T , et al . Inverse energy cascade structure of turbulence in a bubby flow (PIV measurement and results) [J ] . Transactions of the Japan Society of Mechanical Engineers , 2008 , 43 ( 632 ): 1339 - 1346 .
Funfschilling D , Li H Z . Flow of non-Newtonian fluids around bubbles: PIV measurements and birefringence visualisation [J ] . Chemical Engineering Science , 2001 , 56 ( 3 ): 1137 - 1141 .
Westerweel J , Elsinga G E , Adrian R J . Particle image velocimetry for complex and turbulent flows [J ] . Annual Review of Fluid Mechanics , 2013 , 45 ( 45 ): 409 - 436 .
Elsinga G E , Scarano F , Wieneke B , et al . Tomographic particle image velocimetry [J ] . Experiments in Fluids , 2006 , 41 ( 6 ): 933 - 947 .
王蒙 , 程文 , 孙楠 , 等 . 不同高径比下气液两相流流场结构的实验研究 [J ] . 西安理工大学学报 , 2015 , 31 ( 4 ): 434 - 438 .
Wang M , Cheng W , Sun N , et al . Experimental study of flow structure of gas liquid two-phase flow under different aspect ratio [J ] . Journal of Xi'an University of Technology , 2015 , 31 ( 4 ): 434 - 438 .
王云兴 , 汪兵 , 任聪静 , 等 . 气液搅拌釜泛点转速的声波测量 [J ] . 化工学报 , 2009 , 60 ( 5 ): 1148 - 1155 .
Wang Y X , Wang B , Ren C J , et al . Identification of flooding-loading transition in stirred vessel based on acoustic method [J ] . CIESC Journal , 2009 , 60 ( 5 ): 1148 - 1155 .
董志勇 . 射流力学 [M ] . 北京 : 科学出版社 , 2005 : 27 - 29 .
Dong Z Y . Jet Flow Mechanics [M ] . Beijing : Science Press , 2005 : 27 - 29 .
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