Preparation and humidity-controlling characterization of composite CMC-g-PAM/PAAS porous resin by twice foaming method
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Preparation and humidity-controlling characterization of composite CMC-g-PAM/PAAS porous resin by twice foaming method
CIESC JournalIssue 12, (2010)
作者机构:
1. 浙江理工大学先进纺织材料与制备技术教育部重点实验室,浙江,杭州,310018
2. 中国丝绸博物馆,浙江,杭州,310002
3. 浙江理工大学文物保护材料研究室,浙江,杭州,310018
作者简介:
基金信息:
DOI:
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Online First:05 December 2010,
Published:05 December 2010
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杨海亮. Preparation and humidity-controlling characterization of composite CMC-g-PAM/PAAS porous resin by twice foaming method[J]. CIESC Journal, 2010, (12).
DOI:
杨海亮. Preparation and humidity-controlling characterization of composite CMC-g-PAM/PAAS porous resin by twice foaming method[J]. CIESC Journal, 2010, (12).DOI:
Preparation and humidity-controlling characterization of composite CMC-g-PAM/PAAS porous resin by twice foaming method
摘要
Abstract
According to the structural design of porous resin
CMC-g-PAM/PAAS porous resin was prepared by the twice foaming method.The morphology and structure properties of the resin were characterized by thermogravimetry (TG)
scanning electron microscopy (SEM)
X-ray diffractometer (XRD)
Fourier transform infrared spectroscopy (FTIR) and nitrogen adsorption.Humidity-controlling capability and maximum moisture content of the porous resin were tested under high humidity and low humidity conditions.Humidity-controlling capability was investigated at changing absolute humidity and temperature.The results showed that when aluminum chloride was 2.5%(mass) of the acrylamide monomer
the porous resin showed a humidity-controlling range of 57.5%—62.5%
its maximum moisture content was 122% of its own mass.The porous resin was able to maintain relative humidity in the range of 57.5%—62.5% also in the case of changing absolute humidity. The porous resin reached equilibrium humidity in less than 1 h at 40℃ and in less than 3 h at 10℃.