REDUCTION PROCESS OF 3,4,5-TRIMETHOXYBENZALDEHYDE OVER Pd/C CATALYST

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- REDUCTION PROCESS OF 3,4,5-TRIMETHOXYBENZALDEHYDE OVER Pd/C CATALYST
- CIESC Journal Issue 2, (2002)
- 作者机构：
  
  中国矿业大学化学工程学院
- 作者简介：
- 基金信息：
- DOI：
  CLC：
- Online First：25 February 2002，
  
  Published：25 February 2002
- 稿件说明：
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JI Yafei, XU Xin, ZONG Zhimin, et al. REDUCTION PROCESS OF 3,4,5-TRIMETHOXYBENZALDEHYDE OVER Pd/C CATALYST[J]. CIESC Journal, 2002, (2).
DOI：

JI Yafei, XU Xin, ZONG Zhimin, et al. REDUCTION PROCESS OF 3,4,5-TRIMETHOXYBENZALDEHYDE OVER Pd/C CATALYST[J]. CIESC Journal, 2002, (2). DOI：

Trimethoxybenzaldehyde (TMB) was hydrogenated over Pd/C in H 2-AcOH

in H 2-MeOH and in NH 2NH 2-PhMe system respectively.In Pd/C-TMB-H 2-AcOH system

TMB was reduced into 3

5-trimethoxytoluene (TMT) via 3

5-trimethoxybenzyl acetate and (1′-hydroxy)ethyl (3

5-trimethoxy)benzyl ether.In Pd/C-TMB-H 2-MeOH system

TMB was reduced into TMT via 3

5-trimethoxybenzyl alcohol

methyl(3

5-trimethoxy)benzyl ether and bis(3

5-trimethoxy)benzyl ether.In Pd/C-TMB-NH 2NH 2-PhMe system

TMB was reduced into TMT directly with mild manner and higher selectivity.

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