Oxidative esterification of methacrolein to methyl methacrylate

ZHAO Wei; LI Zengxi; ZHANG Suojiang; PANG Haijian; DONG Haifeng; ZHANG Xiangping

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Oxidative esterification of methacrolein to methyl methacrylate

更新时间：2025-12-10

- Oxidative esterification of methacrolein to methyl methacrylate
- CIESC Journal Issue 9, Pages: 1690-1693(2005)
- 作者机构：
  
  1. 中国科学院过程工程研究所绿色化学与技术课题组,北京,100080
  2. 中国科学院研究生院,北京,100039
  3. 哈尔滨工程大学化工学院,黑龙江,哈尔滨,150001
- 作者简介：
- 基金信息：
- DOI：
  CLC：
- Online First：25 September 2005，
  
  Published：25 September 2005
- 稿件说明：
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ZHAO Wei, LI Zengxi, ZHANG Suojiang, et al. Oxidative esterification of methacrolein to methyl methacrylate[J]. CIESC Journal, 2005, (9): 1690-1693.
DOI：

ZHAO Wei, LI Zengxi, ZHANG Suojiang, et al. Oxidative esterification of methacrolein to methyl methacrylate[J]. CIESC Journal, 2005, (9): 1690-1693. DOI：

摘要

Abstract

Supported multi-metal catalyst was prepared by impregnation.A variety of factors such as reaction temperature

feedstock ratio

alkali concentration

catalyst concentration and antipolymerizer concentration were systematically investigated in terms of their effects on the oxidative esterification reaction for methyl methacrylate production from methacrolein.The experimental results showed that under the condition of temperature 333 K，methanol/methacrolein ratio 97∶1(molar ratio)，NaOH concentration 0.001 g8226;ml-1 and catalyst concentration 0.02 g8226;ml-1

methacrolein conversion and methyl methacrylate selectivity were about 100% and 71.4% respectively

after 30 min reaction.

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Related Author

ZHANG Suojiang

ZHANG Xiangping

ZHAO Wei

CHENG Weiguo

WANG Zhengping

LI Zengxi

DONG Haifeng

MA Luming

Related Institution

同济大学环境科学与工程学院，污染控制与资源化研究国家重点实验室

浙江工业大学化工与材料学院

南京工业大学生物与制药工程学院

华南理工大学环境科学与工程学院

北京工业大学绿色化学与精细化工研究所

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